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dc.contributor.authorKamieniak, Joanna-
dc.contributor.authorBernalte Morgado, Elena María-
dc.contributor.authorFoster, Christopher W.-
dc.contributor.authorDoyle, Aidan M.-
dc.contributor.authorKelly, Peter J.-
dc.contributor.authorBanks, Craig E.-
dc.date.accessioned2018-05-04T11:59:33Z-
dc.date.available2018-05-04T11:59:33Z-
dc.date.issued2016-
dc.identifier.urihttp://hdl.handle.net/10662/7389-
dc.description.abstractA novel procedure for the synthesis of both hydroxyapatite (HAP) and palladium doped HAP via a wet chemical precipitation method is described herein. X-ray Diffraction (XRD), Raman Spectroscopy, Scanning Electron Microscopy (SEM) with Energy Dispersive X-ray Spectroscopy (EDS) and Fourier Transform Infrared (FT-IR) Spectroscopy are utilised to characterise the synthesized material’s morphology, structure and crystallinity. The developed synthetic protocol produces high purity HAP with an average yield of 83.7 (± 0.10)% and an average particle size of 58.2 (± 0.98) nm, such synthesis has been achieved at room temperature and within a time period of less than 24 h. Additionally, in order to enhance the overall conductivity of the material, a range of Pd (2, 4 and 6 wt %) metal doped HAP has been synthesised, characterised and, for the first time, applied towards the competitive electrocatalytic detection of hydrazine, exhibiting a linear range of 50–400 μ M with a limit of detection (3 σ) of 30 μ M.es_ES
dc.format.extent15 p.es_ES
dc.language.isoenges_ES
dc.publisherMDPIes_ES
dc.rightsAtribución-NoComercial-SinDerivadas 3.0 España*
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/3.0/es/*
dc.subjectHidroxiapatitaes_ES
dc.subjectPaladioes_ES
dc.subjectSíntesises_ES
dc.subjectHidracinaes_ES
dc.subjectAplicación electroquímicaes_ES
dc.subjectHydroxyapatitees_ES
dc.subjectPalladiumes_ES
dc.subjectSynthesises_ES
dc.subjectHydrazinees_ES
dc.subjectElectrochemical applicationes_ES
dc.titleHigh yield synthesis of hydroxyapatite (HAP) and Palladium Doped HAP via a wet chemical synthetic routees_ES
dc.typearticlees_ES
dc.description.versionpeerReviewedes_ES
dc.rights.accessRightsopenAccesses_ES
dc.subject.unesco2210.05 Electroquímicaes_ES
dc.subject.unesco3303.09 Operaciones Electroquímicases_ES
dc.subject.unesco2301 Química Analíticaes_ES
dc.identifier.bibliographicCitationKamieniak, J.; Bernalte Morgado, E. M.; Foster, C. W.; Doyle, A. M.; Kelly P. J. y Banks, C. E. (2016). High yield synthesis of hydroxyapatite (HAP) and Palladium Doped HAP via a wet chemical synthetic route. Catalysts, 6, 8, 119. ESSN 2073-4344es_ES
dc.type.versionpublishedVersiones_ES
dc.contributor.affiliationManchester Metropolitan University. UKes_ES
dc.contributor.affiliationUniversidad de Extremadura. Departamento de Química Analíticaes_ES
dc.relation.publisherversionhttp://www.mdpi.com/2073-4344/6/8/119es_ES
dc.identifier.doi10.3390/catal6080119-
dc.identifier.publicationtitleCatalystses_ES
dc.identifier.publicationissue8es_ES
dc.identifier.publicationfirstpage1es_ES
dc.identifier.publicationlastpage15es_ES
dc.identifier.publicationvolume6, 119es_ES
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