Identificador persistente para citar o vincular este elemento:
http://hdl.handle.net/10662/7389
Registro completo de Metadatos
Campo DC | Valor | idioma |
---|---|---|
dc.contributor.author | Kamieniak, Joanna | - |
dc.contributor.author | Bernalte Morgado, Elena María | - |
dc.contributor.author | Foster, Christopher W. | - |
dc.contributor.author | Doyle, Aidan M. | - |
dc.contributor.author | Kelly, Peter J. | - |
dc.contributor.author | Banks, Craig E. | - |
dc.date.accessioned | 2018-05-04T11:59:33Z | - |
dc.date.available | 2018-05-04T11:59:33Z | - |
dc.date.issued | 2016 | - |
dc.identifier.uri | http://hdl.handle.net/10662/7389 | - |
dc.description.abstract | A novel procedure for the synthesis of both hydroxyapatite (HAP) and palladium doped HAP via a wet chemical precipitation method is described herein. X-ray Diffraction (XRD), Raman Spectroscopy, Scanning Electron Microscopy (SEM) with Energy Dispersive X-ray Spectroscopy (EDS) and Fourier Transform Infrared (FT-IR) Spectroscopy are utilised to characterise the synthesized material’s morphology, structure and crystallinity. The developed synthetic protocol produces high purity HAP with an average yield of 83.7 (± 0.10)% and an average particle size of 58.2 (± 0.98) nm, such synthesis has been achieved at room temperature and within a time period of less than 24 h. Additionally, in order to enhance the overall conductivity of the material, a range of Pd (2, 4 and 6 wt %) metal doped HAP has been synthesised, characterised and, for the first time, applied towards the competitive electrocatalytic detection of hydrazine, exhibiting a linear range of 50–400 μ M with a limit of detection (3 σ) of 30 μ M. | es_ES |
dc.format.extent | 15 p. | es_ES |
dc.language.iso | eng | es_ES |
dc.publisher | MDPI | es_ES |
dc.rights | Atribución-NoComercial-SinDerivadas 3.0 España | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/3.0/es/ | * |
dc.subject | Hidroxiapatita | es_ES |
dc.subject | Paladio | es_ES |
dc.subject | Síntesis | es_ES |
dc.subject | Hidracina | es_ES |
dc.subject | Aplicación electroquímica | es_ES |
dc.subject | Hydroxyapatite | es_ES |
dc.subject | Palladium | es_ES |
dc.subject | Synthesis | es_ES |
dc.subject | Hydrazine | es_ES |
dc.subject | Electrochemical application | es_ES |
dc.title | High yield synthesis of hydroxyapatite (HAP) and Palladium Doped HAP via a wet chemical synthetic route | es_ES |
dc.type | article | es_ES |
dc.description.version | peerReviewed | es_ES |
dc.rights.accessRights | openAccess | es_ES |
dc.subject.unesco | 2210.05 Electroquímica | es_ES |
dc.subject.unesco | 3303.09 Operaciones Electroquímicas | es_ES |
dc.subject.unesco | 2301 Química Analítica | es_ES |
dc.identifier.bibliographicCitation | Kamieniak, J.; Bernalte Morgado, E. M.; Foster, C. W.; Doyle, A. M.; Kelly P. J. y Banks, C. E. (2016). High yield synthesis of hydroxyapatite (HAP) and Palladium Doped HAP via a wet chemical synthetic route. Catalysts, 6, 8, 119. ESSN 2073-4344 | es_ES |
dc.type.version | publishedVersion | es_ES |
dc.contributor.affiliation | Manchester Metropolitan University. UK | es_ES |
dc.contributor.affiliation | Universidad de Extremadura. Departamento de Química Analítica | es_ES |
dc.relation.publisherversion | http://www.mdpi.com/2073-4344/6/8/119 | es_ES |
dc.identifier.doi | 10.3390/catal6080119 | - |
dc.identifier.publicationtitle | Catalysts | es_ES |
dc.identifier.publicationissue | 8 | es_ES |
dc.identifier.publicationfirstpage | 1 | es_ES |
dc.identifier.publicationlastpage | 15 | es_ES |
dc.identifier.publicationvolume | 6, 119 | es_ES |
Colección: | DQUAN - Artículos |
Archivos
Archivo | Descripción | Tamaño | Formato | |
---|---|---|---|---|
catal6080119.pdf | 2,9 MB | Adobe PDF | Descargar |
Este elemento está sujeto a una licencia Licencia Creative Commons